产品名称：	HH-624毛细管柱 测定药用聚乙烯醇中甲醇溶剂残留量
产品型号：	HH-624毛细管柱
品牌：	1941
产品数量：
产品单价：	面议
日期:	2024-06-16

HH-624毛细管柱 测定药用聚乙烯醇中甲醇溶剂残留量的详细资料

测定药用聚乙烯醇中甲醇溶剂残留量
测定药用聚乙烯醇中甲醇溶剂残留量 详细信息：

名称：毛细管色谱柱

固定相：6% 氰丙基苯基／94% 二甲基聚硅氧烷
极性：弱极性到中等极性固定相
相当于 USP 固定相 G43

型号：HH-624

规格：30m*0.53mm*3.0um

应用：药用辅料聚乙烯醇质量标准

浩瀚色谱（山东）应用技术开发有限公司研发一种测定聚乙烯醇树脂类物质中挥发性组分含量的方法，采用了全蒸发顶空气相色谱法分析，具体步骤为：将聚乙烯醇树脂类物质0.1克～0.5克用20毫升顶空瓶密封，放入顶空进样器中，在115℃～125℃的条件下加热85分钟～95分钟使挥发性组分完全蒸发，采用气相色谱法分析，记录挥发性组分的谱图，然后用标准回归曲线法计算挥发性组分的含量；分析条件为：采用HH-624型色谱柱，采用FID检测器，柱温40℃，检测器温度200℃；进样器温度150℃。该方法分析数据重现性好，分析数据准确，具有操作简单、方便、分析速度快、灵敏度高的特点，样品中挥发性组分分离效果好。


测定药用聚乙烯醇中甲醇溶剂残留量 测试谱图：




Determination of residual methanol solvent in medicinal polyvinyl alcohol
Determination of residual methanol solvent in medicinal polyvinyl alcohol. Details:

Name: Capillary Chromatographic Column

Stationary phase: 6% cyanopropyl phenyl/94% dimethyl polysiloxane
Polarity: weak to medium polarity stationary phase
Equivalent to USP stationary phase G43

Model: HH-624

Specification: 30m*0.53mm*3.0um

Application: Quality standard of polyvinyl alcohol for pharmaceutical excipients



Haohan Chromatography (Shandong) Applied Technology Development Co., Ltd. has developed a method to determine the content of volatile components in polyvinyl alcohol resins. The method uses pervaporation headspace gas chromatography to analyze. The specific steps are: 0.1g～0.5g of the substance is sealed with a 20ml headspace bottle, put into the headspace sampler, heated at 115℃～125℃ for 85 minutes～95 minutes to completely evaporate the volatile components, using gas chromatography Analyze and record the spectra of volatile components, and then use the standard regression curve method to calculate the content of volatile components; the analysis conditions are: use HH-624 chromatographic column, use FID detector, column temperature 40℃, detector temperature 200℃; The temperature of the injector is 150℃. The method has good reproducibility of analysis data, accurate and reliable analysis data, simple operation, convenient operation, fast analysis speed, high sensitivity, and good separation effect of volatile components in the sample.


Determination of residual methanol solvent in medicinal polyvinyl alcohol Test spectrum: